高分子多孔微球填充柱分析微量水分，芝麻香白酒，3-甲硫基丙醇，粗苯，三苯，水分，噻吩，變壓器油，多氯聯(lián)苯，植物油，6號溶劑殘留，醫(yī)療器械，環(huán)氧乙烷，三甲胺，氨

高分子多孔微球填充柱分析微量水分
高分子多孔微球填充柱分析微量水分 詳細(xì)信息：

編號：20221210001
型號：高分子多孔微球填充柱
規(guī)格：1m*3.2mm，60-80目
*高使用溫度：270°C

應(yīng)用：安捷倫7820A，7890B
GB 18582-2020建筑用墻面涂料中有害物質(zhì)限量
GB 24408-2009 建筑用外墻涂料中有害物質(zhì)限量
GB 33372-2020 膠粘劑揮發(fā)性有機(jī)化合物限量
GB18582—2001室內(nèi)裝飾裝修材料 內(nèi)墻涂料中有害物質(zhì)限量
GB18582-2008室內(nèi)裝飾裝修材料內(nèi)墻涂料中有害物質(zhì)限量
GBT333722016膠粘劑揮發(fā)性有機(jī)化合物限量

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司通過改善萃取試劑,優(yōu)化相對校正因子,超聲萃取時間,進(jìn)樣體積等影響因素,建立簡便,準(zhǔn)確的氣相色譜法檢測水性內(nèi)墻涂料中水分含量的方法.實驗方法優(yōu)的分析條件為:0.2 g樣品加入2 mL異丙醇(0.1 g/mL)DMF內(nèi)標(biāo)溶液,恒溫23℃超聲萃取10 min,恒溫23℃離心5 min,1.0μL上清液進(jìn)氣相色譜分析.采用內(nèi)標(biāo)法,應(yīng)用校正曲線計算內(nèi)墻涂料中水分含量.水分含量校準(zhǔn)曲線方程為Y=2.43X+0.049,相關(guān)系數(shù)R2=0.999 8.相對標(biāo)準(zhǔn)偏差(RSD)為0.22%～0.68%(n=6),回收率為98%～108%.實驗方法提高了萃取效率,縮短了分析時間,減少了實驗誤差,具有良好的重現(xiàn)性和準(zhǔn)確性.

高分子多孔微球填充柱分析微量水分測試譜圖：



Analysis of trace moisture in porous polymer microsphere packed column

Detailed information of micro moisture analysis by polymer porous microsphere packed column:




No.: 20221210001

Model: polymer porous microsphere packed column

Specification: 1m * 3.2mm, 60-80 mesh

*High service temperature: 270 ° C



Application: Agilent 7820A, 7890B

GB 18582-2020 Limit of Harmful Substances in Wall Coatings for Building

GB 24408-2009 Limit of Harmful Substances in Exterior Wall Coatings for Building

GB 33372-2020 Limit of Volatile Organic Compounds in Adhesives

GB18582-2001 Indoor Decoration Materials Limit of Harmful Substances in Interior Wall Coatings

GB18582-2008 Indoor Decoration Materials Limit of Harmful Substances in Interior Wall Coatings

GBT333722016 Limit of Volatile Organic Compounds in Adhesives




Haohan Chromatographic (Shandong) Application Technology Development Co., Ltd. established a simple and accurate gas chromatographic method to detect the water content in water-based interior wall coatings by improving the extraction reagent, optimizing the relative correction factor, ultrasonic extraction time, sample injection volume and other influencing factors. The optimal analysis conditions of the experimental method are: 0.2 g of sample is added with 2 mL of isopropanol (0.1 g/mL) DMF internal standard solution, ultrasonic extraction at 23 ℃ for 10 minutes, centrifugation at 23 ℃ for 5 minutes, and 1.0 μ L supernatant gas chromatographic analysis. The internal standard method is used to calculate the moisture content in the interior wall coating by using the calibration curve. The equation of the moisture content calibration curve is Y=2.43X+0.049, and the correlation coefficient R2=0.999 8. The relative standard deviation (RSD) is 0.22% ～ 0.68% (n=6), and the recovery is 98% ～ 108% The experimental method improves the extraction efficiency, shortens the analysis time, reduces the experimental error, and has good reproducibility and accuracy



Micro moisture test spectrogram of polymer porous microsphere packed column analysis: